Technology Process of C23H17BN2O6
There total 2 articles about C23H17BN2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-Aminophenylboronic acid;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine;
With
N-ethylmorpholine;; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 20h;
Inert atmosphere;
With
trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
for 0.0166667h;
Inert atmosphere;
DOI:10.1039/c2cc33559j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethylmorpholine;; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere
1.2: 12 h / 20 °C / Cooling with ice; Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere; Cooling with ice
3.1: PS-DEAM / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3.2: 20 h / 20 °C / Inert atmosphere
3.3: 0.02 h / Inert atmosphere
With
N-ethylmorpholine;; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33559j
![N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine](/Databaselist/images/loading.webp)
