[OsCl(NC(CH₃)2)(P(CH(CH₃)2)3)2(CCHC(CH₃)(C₆H₅))]⁽¹⁺⁾*CF₃SO₃^(1-)=[OsCl(P(CH(CH₃)2)3)2(NC(CH₃)2)(CCHC(CH₃)(C₆H₅))]CF₃SO₃

Base Information

• Chemical Name: [OsCl(NC(CH₃)2)(P(CH(CH₃)2)3)2(CCHC(CH₃)(C₆H₅))]⁽¹⁺⁾*CF₃SO₃^(1-)=[OsCl(P(CH(CH₃)2)3)2(NC(CH₃)2)(CCHC(CH₃)(C₆H₅))]CF₃SO₃
• CAS No.: 355018-12-1
• Molecular Formula: CF₃O₃S*C₃₁H₅₇ClNOsP₂
• Molecular Weight: 880.471

Synonyms:

Chemical Property of [OsCl(NC(CH₃)2)(P(CH(CH₃)2)3)2(CCHC(CH₃)(C₆H₅))]⁽¹⁺⁾*CF₃SO₃^(1-)=[OsCl(P(CH(CH₃)2)3)2(NC(CH₃)2)(CCHC(CH₃)(C₆H₅))]CF₃SO₃

Chemical Property:

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Safty Information:

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Useful:

Technology Process of [OsCl(NC(CH₃)2)(P(CH(CH₃)2)3)2(CCHC(CH₃)(C₆H₅))]⁽¹⁺⁾*CF₃SO₃^(1-)=[OsCl(P(CH(CH₃)2)3)2(NC(CH₃)2)(CCHC(CH₃)(C₆H₅))]CF₃SO₃

There total 1 articles about [OsCl(NC(CH₃)2)(P(CH(CH₃)2)3)2(CCHC(CH₃)(C₆H₅))]⁽¹⁺⁾*CF₃SO₃^(1-)=[OsCl(P(CH(CH₃)2)3)2(NC(CH₃)2)(CCHC(CH₃)(C₆H₅))]CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2-Phenyl-3-butyn-2-ol (127-66-2) + Os(H)Cl2(P(CH(CH3)2)3)2(NC(CH3)2) (288324-68-5) + silver trifluoromethanesulfonate (2923-28-6) → [OsCl(NC(CH3)2)(P(CH(CH3)2)3)2(CCHC(CH3)(C6H5))](1+)*CF3SO3(1-)=[OsCl(P(CH(CH3)2)3)2(NC(CH3)2)(CCHC(CH3)(C6H5))]CF3SO3 (355018-12-1)

Guidance literature:

In dichloromethane; acetone; byproducts: AgCl, H2O; using Schlenk techniques; treatment of soln. of (OsHCl2(P(CH(CH3)2)3)2(NCMe2) in CH2Cl2 and acetone with Ag(CF3SO3); stirring for 3 h; filtration, addn. of 2-phenyl-3-butyn-2-ol, stirring for 1 h at room temp.; concn. of solvent, addn. of diethyl ether, pptn., washing with diethyl ether, drying in vac., elem. anal.;

DOI:10.1021/om0101386

Reference yield: 72.0%

[OsCl(NC(CH3)2)(P(CH(CH3)2)3)2(CCHC(CH3)(C6H5))](1+)*CF3SO3(1-)=[OsCl(P(CH(CH3)2)3)2(NC(CH3)2)(CCHC(CH3)(C6H5))]CF3SO3 (355018-12-1) + methyllithium (917-54-4) → [OsCl(P(CH(CH3)2)3)2(NC(CH3)2)(CCHC(C6H5)CH2)]

Guidance literature:

In tetrahydrofuran; diethyl ether; byproducts: CH4, Li(CF3SO3); using Schlenk techniques; treatment of soln. of (OsCl(P(CH(CH3)2)3)2(NCMe2)(CCHCMePh))(CF3SO3) in THF with soln. of MeLi in diethyl ether at room temp. for 5 min; concn. of solvent to dryness, addn. of toluene, filtration, removal of toluene, addn. of methanol at -78°C, pptn., washing with cold methanol and pentane, drying in vac., elem. anal.;

DOI:10.1021/om0101386

upstream raw materials:

2-Phenyl-3-butyn-2-ol

Os(H)Cl₂(P(CH(CH₃)2)3)2(NC(CH₃)2)

silver trifluoromethanesulfonate

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