N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

Base Information

Chemical Name:N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate
CAS No.:221277-32-3
Molecular Formula:C₂₀H₂₉N₈O₁₄P₃
Molecular Weight:698.417
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

Chemical Property:

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Technology Process of N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

There total 5 articles about N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2627-69-2
AICA riboside

: 221277-32-3
N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / NaOH / methanol / 3 h / 180 °C / 16501.3 Torr

2: H₂O₂ / D₂O / 1 h / 0 °C

3: 2.5 h / 135 °C

4: 41 percent / Na₂CO₃ / dimethylformamide / 4.5 h / 50 °C

5: 1.) (MeO)3PO, POCl₃, 2.) tributylammonium imidodiphosphate, Bu₃N / 1.) 0 deg C, 45 min, 2.) DMF, 0 deg C, 1.5 min

With trimethyl phosphite; sodium hydroxide; tributyl-amine; tri-n-butylammonium salt of imidodiphosphate; dihydrogen peroxide; sodium carbonate; trichlorophosphate; In methanol; water-d2; N,N-dimethyl-formamide;
DOI:10.1080/15257779908043072

Reference yield:

: 13389-80-5
sodium salt of 2-mercaptoinosine

: 221277-32-3
N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂O₂ / D₂O / 1 h / 0 °C

2: 2.5 h / 135 °C

3: 41 percent / Na₂CO₃ / dimethylformamide / 4.5 h / 50 °C

4: 1.) (MeO)3PO, POCl₃, 2.) tributylammonium imidodiphosphate, Bu₃N / 1.) 0 deg C, 45 min, 2.) DMF, 0 deg C, 1.5 min

With trimethyl phosphite; tributyl-amine; tri-n-butylammonium salt of imidodiphosphate; dihydrogen peroxide; sodium carbonate; trichlorophosphate; In water-d2; N,N-dimethyl-formamide;
DOI:10.1080/15257779908043072

Reference yield:

: 221277-19-6
N-2-(2-aminoethyl)guanosine

: 221277-32-3
N-2-(2-N'-methylanthraniloylaminoethyl)guanosine-5'-(β,γ-imido)triphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / Na₂CO₃ / dimethylformamide / 4.5 h / 50 °C

2: 1.) (MeO)3PO, POCl₃, 2.) tributylammonium imidodiphosphate, Bu₃N / 1.) 0 deg C, 45 min, 2.) DMF, 0 deg C, 1.5 min

With trimethyl phosphite; tributyl-amine; tri-n-butylammonium salt of imidodiphosphate; sodium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1080/15257779908043072