Technology Process of C11H11F2N3O2
There total 5 articles about C11H11F2N3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethylamino-sulfur trifluoride / dichloromethane / -30 - 20 °C
2: ozone; dimethylsulfide / dichloromethane
With
dimethylsulfide; diethylamino-sulfur trifluoride; ozone;
In
dichloromethane;
DOI:10.1021/cb5003416
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride; 4-methyl-morpholine / dichloromethane; dimethyl sulfoxide / -78 °C
2: diethylamino-sulfur trifluoride / dichloromethane / -30 - 20 °C
3: ozone; dimethylsulfide / dichloromethane
With
4-methyl-morpholine; oxalyl dichloride; dimethylsulfide; diethylamino-sulfur trifluoride; ozone;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1021/cb5003416
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide; ammonium chloride; methanol / water
2: oxalyl dichloride; 4-methyl-morpholine / dichloromethane; dimethyl sulfoxide / -78 °C
3: diethylamino-sulfur trifluoride / dichloromethane / -30 - 20 °C
4: ozone; dimethylsulfide / dichloromethane
With
4-methyl-morpholine; methanol; sodium azide; oxalyl dichloride; dimethylsulfide; diethylamino-sulfur trifluoride; ammonium chloride; ozone;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/cb5003416