tris(p-chlorophenyl)antimony dibromide

Base Information

• Chemical Name: tris(p-chlorophenyl)antimony dibromide
• CAS No.: 61184-33-6
• Molecular Formula: C₁₈H₁₂Br₂Cl₃Sb
• Molecular Weight: 616.21
• Mol file: 61184-33-6.mol

Synonyms:

Chemical Property of tris(p-chlorophenyl)antimony dibromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tris(p-chlorophenyl)antimony dibromide

There total 3 articles about tris(p-chlorophenyl)antimony dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

tris(4-chlorophenyl)stilbane (6944-25-8) → tris(p-chlorophenyl)antimony dibromide (61184-33-6,91002-41-4)

Guidance literature:

With bromine; In Petroleum ether; slow addn. of bromine to an ice-cooled Sb compd. soln.; stirring, 3-4 h; filtration; recrystn. (petroleum ether), elem. anal.;

Reference yield:

4-chlorophenylmagnesium chloride (51833-36-4) → (4-ClC6H4)3SbBr2 (61184-33-6,91002-41-4)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: ethanol

In diethyl ether; ethanol;

Reference yield:

(4-chlorphenyl)magnesium bromide (873-77-8) → (4-ClC6H4)3SbBr2 (61184-33-6,91002-41-4)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: ethanol

In diethyl ether; ethanol;

upstream raw materials:

4-chlorophenylmagnesium chloride

(4-chlorphenyl)magnesium bromide

tris(4-chlorophenyl)stilbane

Downstream raw materials:

(ClC₆H₄)3Sb(ON(CO)2C₆H₆O)2

(ClC₆H₄)3Sb(ON(CO)2C₆H₈O)2

Refernces