Tris(p-chlorophenyl)stibine

Base Information

Chemical Name:Tris(p-chlorophenyl)stibine
CAS No.:6944-25-8
Molecular Formula:C18H12 Cl3 Sb
Molecular Weight:456.402
Hs Code.:
NSC Number:55918
DSSTox Substance ID:DTXSID00288467

Synonyms:Tris(p-chlorophenyl)stibine;6944-25-8;tris(4-chlorophenyl)stibane;Stibine, tris(p-chlorophenyl)-;Stibine, tris(4-chlorophenyl)-;NSC55918;tris-(p-chlorophenyl)antimony;SCHEMBL5331495;Stibene, tris(p-chlorophenyl)-;DTXSID00288467;NSC-55918

Suppliers and Price of Tris(p-chlorophenyl)stibine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Tris(p-chlorophenyl)stibine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:453.90427
Heavy Atom Count:22
Complexity:275

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1Cl)[Sb](C2=CC=C(C=C2)Cl)C3=CC=C(C=C3)Cl

Technology Process of Tris(p-chlorophenyl)stibine

There total 2 articles about Tris(p-chlorophenyl)stibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.5%

: 10025-91-9
antimony(III) chloride

: 51833-36-4
4-chlorophenylmagnesium chloride

: 6944-25-8
tris(4-chlorophenyl)stilbane

Guidance literature:: In diethyl ether; treating with water, concn., adding ethanol;

Reference yield:

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 6944-25-8
tris(4-chlorophenyl)stilbane

Guidance literature:: With diethyl ether; antimony(III) chloride;
DOI:10.1039/jr9470001568

Reference yield: 92.0%

: 6944-25-8
tris(4-chlorophenyl)stilbane

: 126-30-7
2,2-Dimethyl-1,3-propanediol

2-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaborinane: 827605-29-8
2-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaborinane

Guidance literature:: tris(4-chlorophenyl)stilbane; With boron trichloride; In dichloromethane; at 0 ℃; for 2h;

With methanol; at 20 ℃; for 0.5h;

2,2-Dimethyl-1,3-propanediol; In methanol; at 20 ℃; for 1h;
DOI:10.1246/cl.2006.1402