Fe(OCH₂CH₂CH₂CONH(CH₂)6O₃CH₃)4(C₆H₃)2C₂₀H₉N₄(C₆H₃CH₃(O(CH₂)6C₃H₃N₂))⁽¹⁺⁾*Cl^(1-)=C₉₂H₁₂₄FeN₁₀O₂₁Cl

Base Information

• Chemical Name: Fe(OCH₂CH₂CH₂CONH(CH₂)6O₃CH₃)4(C₆H₃)2C₂₀H₉N₄(C₆H₃CH₃(O(CH₂)6C₃H₃N₂))⁽¹⁺⁾*Cl^(1-)=C₉₂H₁₂₄FeN₁₀O₂₁Cl
• CAS No.: 331273-61-1
• Molecular Formula: C₉₂H₁₂₄FeN₁₀O₂₁*Cl
• Molecular Weight: 1797.35

Synonyms:

Chemical Property of Fe(OCH₂CH₂CH₂CONH(CH₂)6O₃CH₃)4(C₆H₃)2C₂₀H₉N₄(C₆H₃CH₃(O(CH₂)6C₃H₃N₂))⁽¹⁺⁾*Cl^(1-)=C₉₂H₁₂₄FeN₁₀O₂₁Cl

Chemical Property:

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Safty Information:

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Technology Process of Fe(OCH₂CH₂CH₂CONH(CH₂)6O₃CH₃)4(C₆H₃)2C₂₀H₉N₄(C₆H₃CH₃(O(CH₂)6C₃H₃N₂))⁽¹⁺⁾*Cl^(1-)=C₉₂H₁₂₄FeN₁₀O₂₁Cl

There total 2 articles about Fe(OCH₂CH₂CH₂CONH(CH₂)6O₃CH₃)4(C₆H₃)2C₂₀H₉N₄(C₆H₃CH₃(O(CH₂)6C₃H₃N₂))⁽¹⁺⁾*Cl^(1-)=C₉₂H₁₂₄FeN₁₀O₂₁Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

(SP-5-13)-([tetrakis[2-[2-(2-methoxyethoxy)ethoxy]ethyl] 4,4',4'',4'''-[10-(3-[[6-(1H-imidazol-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-1,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis[butanamido]](2-)-N(21),N(22),N(23),N(24), N(3))zinc(II) (331273-60-0) + iron(II) chloride → Fe(OCH2CH2CH2CONH(CH2)6O3CH3)4(C6H3)2C20H9N4(C6H3CH3(O(CH2)6C3H3N2))(1+)*Cl(1-)=C92H124FeN10O21Cl (331273-61-1)

Guidance literature:

With CF₃COOH; 2,6-lutidine; In chloroform; Zn-complex in CHCl3 was reacted with CF3CO2H at 0°C, stirred at room temp. for 5 min, titrated with 2,6-lutidine, washed with H2O, aq. phase was removed, solvent was distilled off under vac., dried under vac. for 2 h, dissolved in THF; 2,6-lutidine was added, refluxed for 15 min, treated with FeCl2, refluxed for 2 h, cooled to room temp., exposed to air for 30 min, filtered, concd. in vacuo, dried under vac., dissolved in CHCl3, HCl in CHCl3, stirred at room temp. for 5 min, evapd.;

DOI:10.1002/1522-2675(200202)85:2<599::AID-HLCA599>3.0.CO;2-V

Reference yield: 49.0%

hydrogenchloride (7647-01-0,15364-23-5) + (SP-5-13)-([tetrakis[2-[2-(2-methoxyethoxy)ethoxy]ethyl] 4,4',4'',4'''-[10-(3-[[6-(1H-imidazol-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-1,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis[butanamido]](2-)-N(21),N(22),N(23),N(24), N(3))zinc(II) (331273-60-0) + iron(II) chloride → FeClC20N4H9(CH3C6H3OC6H12C3N2H3)[C6H3[OC3H6CONH(C2H4O)3CH3]2]2 (331273-61-1)

Guidance literature:

With 2,6-dimethylpyridine; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trifluoroacetic acid; In tetrahydrofuran; demetallation (CF3COOH, CHCl3, 0°C, 5 min); Fe(II) insertion (FeCl2, 2,6-dimethylpyridine, THF, reflux, 2-4 h); autoxidation (HCl, CHCl3,20°C, 5 min), then (1,8-bis(dimethylamino)naphthalene, THF, 20.d egree.C, 15 min); thin layer chromy. (SiO2, CH2Cl2/CH3OH (90/10)), then gel permeation chromy. (Biorad S-X3, CH2Cl2); elem. anal.;

DOI:10.1039/b007611m

Reference yield:

FeClC20N4H9(CH3C6H3OC6H12C3N2H3)[C6H3[OC3H6CONH(C2H4O)3CH3]2]2 (331273-61-1) → FeC20N4H9(CH3C6H3OC6H12C3N2H3)[C6H3[OC3H6CONH(C2H4O)3CH3]2]2 (331273-64-4)

Guidance literature:

With sodium dithionite; In chloroform; water; under Ar; two-phase conditions;

DOI:10.1039/b007611m

upstream raw materials:

hydrogenchloride

(SP-5-13)-([tetrakis[2-[2-(2-methoxyethoxy)ethoxy]ethyl] 4,4',4'',4'''-[10-(3-[[6-(1H-imidazol-1-yl)hexyl]oxy]-4-methylphenyl)-21H,23H-porphine-1,15-diylbis(benzene-2,1,3-triyldioxy)]tetrakis[butanamido]]^(2-)-N⁽²¹⁾,N⁽²²⁾,N⁽²³⁾,N⁽²⁴⁾, N⁽³⁾)zinc(II)

Downstream raw materials:

FeC₂₀N₄H₉(CH₃C₆H₃OC₆H₁₂C₃N₂H₃)[C₆H₃[OC₃H₆CONH(C₂H₄O)3CH₃]2]2

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