((t-Bu)2BnPN)CpTiCl₂

Base Information

Chemical Name:((t-Bu)2BnPN)CpTiCl₂
CAS No.:845783-03-1
Molecular Formula:C₂₀H₃₀Cl₂NPTi
Molecular Weight:434.225
Hs Code.:

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Chemical Property of ((t-Bu)2BnPN)CpTiCl₂

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Technology Process of ((t-Bu)2BnPN)CpTiCl₂

There total 1 articles about ((t-Bu)2BnPN)CpTiCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 845640-19-9
(t-Bu)2BnPNSiMe₃

: 845783-03-1
((t-Bu)2BnPN)CpTiCl₂

Guidance literature:: In toluene; under N2 atm. to soln. CpTiCl3 in toluene (t-Bu)2BnPNSiMe3 was added dropwise at 25°C and stirred for 24 h; volatiles were removed in vacuo, residue was washed with hexane and dried; elem. anal.;
DOI:10.1139/v04-062

Reference yield: 78.0%

: 845783-03-1
((t-Bu)2BnPN)CpTiCl₂

: 75-16-1
methylmagnesium bromide

: 845783-23-5
((t-Bu)2BnPN)CpTiMe₂

Guidance literature:: In diethyl ether; under N2 atm. to slurry Ti complex in Et2O soln. MeMgBr in Et2O was added dropwise at 25°C and stirred for 15 h; solvent was removed in vacuo, residue was extd. with hexane and filtered, solvent was removed in vacuo; elem. anal.;
DOI:10.1139/v04-062