tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate

Base Information

Chemical Name:tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate
CAS No.:1350752-64-5
Molecular Formula:CF₃O₃S*CH₂Cl₂*C₂₄H₂₁MnN₃O₃
Molecular Weight:688.39
Hs Code.:

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Chemical Property of tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate

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Technology Process of tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate

There total 1 articles about tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: bis(2-pyridylmethyl)-4-vinylphenmethylamine

: 14516-54-2
bromopentacarbonylmanganese(I)

: 2923-28-6
silver trifluoromethanesulfonate

: 1350752-64-5
tricarbonylbis(pyridylmethyl)-p-vinylbenzylaminemanganesetriflate methylene dichloride solvate

Guidance literature:: In acetone; byproducts: AgBr; Schlenk technique; Mn(CO)5Br and AgCF3SO3 dissolved in acetone, heated under reflux for 1.5 h, AgBr filtered off, soln. added to soln. of amine,heated under reflux for 1.5 h; solvent evpd., iethyl ether added, filtered, solid washed (diethyl ether), dried (vac.); elem. anal.;
DOI:10.1002/ejic.201100545