⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride

Base Information

• Chemical Name: ⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride
• CAS No.: 1375015-45-4
• Molecular Formula: C₁₃H₁₇N₂*Cl
• Molecular Weight: 237.733
• Mol file: 1375015-45-4.mol

Synonyms:

Chemical Property of ⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of ⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride

There total 1 articles about ⁽¹³⁾C-N-mesityl-N'-methylimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

methylene chloride (74-87-3) + 13C-N-mesitylimidazole (1101127-71-2) → (13)C-N-mesityl-N'-methylimidazolium chloride (1375015-45-4)

Guidance literature:

In tert-butyl methyl ether; acetonitrile; at 120 ℃; for 96h;

DOI:10.1021/om300340w

Reference yield: 79.0%

(13)C-N-mesityl-N'-methylimidazolium chloride (1375015-45-4) + silver(l) oxide (20667-12-3) → ((13)C-N-mesityl-N'-methylimidazolylidene)silver(I) chloride

Guidance literature:

In acetonitrile; under N2; soln. of ligand salt in MeCN and Ag2O placed in flask covered with Al foil; stirred at room temp. for 18 h; filtered through Celite; solid washed with MeCN; MeCN solns. combined; solvent removed under reduced pressure; crystd. from MeCN-ether; elem. anal.;

DOI:10.1021/om300340w

upstream raw materials:

methylene chloride

¹³C-N-mesitylimidazole