Propyl-butyl-phenyl-phosphin

Base Information

• Chemical Name: Propyl-butyl-phenyl-phosphin
• CAS No.: 91954-21-1
• Molecular Formula: C₁₃H₂₁P
• Molecular Weight: 208.284
• Mol file: 91954-21-1.mol

Synonyms:

Chemical Property of Propyl-butyl-phenyl-phosphin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Propyl-butyl-phenyl-phosphin

There total 4 articles about Propyl-butyl-phenyl-phosphin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylphosphane (638-21-1) → Propyl-butyl-phenyl-phosphin (91954-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) 50-56percent aq. KOH / 1) DMSO, 20 deg C, 2) DMSO, 25-30 deg C, 0.5 h

2: 1) K₂CO₃, aq. KOH / 1) HMPA, 20 deg C, 2) HMPA, 45-50 deg C, 2 h

With potassium hydroxide; potassium carbonate;

Reference yield:

butyl(phenyl)phosphine (10251-55-5) + propyl bromide (106-94-5) → Propyl-butyl-phenyl-phosphin (91954-21-1)

Guidance literature:

With potassium hydroxide; potassium carbonate; Yield given. Multistep reaction; 1.) HMPT, 20 deg C, 2.) 45 - 50 deg C, 2 h;

DOI:10.1055/s-1986-31510

Reference yield:

Phenylphosphanyl-methanol → Propyl-butyl-phenyl-phosphin (91954-21-1)

Guidance literature:

upstream raw materials:

1-iodo-butane

1-iodo-propane

bis(hydroxymethyl)phenylphosphine

butyl(phenyl)phosphine

Downstream raw materials:

Methyl-propyl-butyl-phenyl-phosphonium-iodid