PhMe₂GeGePh₃

Base Information

Chemical Name:PhMe₂GeGePh₃
CAS No.:53445-88-8
Molecular Formula:C₂₆H₂₆Ge₂
Molecular Weight:483.672
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PhMe₂GeGePh₃

Chemical Property:

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Technology Process of PhMe₂GeGePh₃

There total 3 articles about PhMe₂GeGePh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1151774-02-5
PhMe₂GeNMe₂

: 2816-43-5
triphenylgermane

: 75-05-8,26809-02-9
acetonitrile

: 53445-88-8
PhMe₂GeGePh₃

Guidance literature:: In acetonitrile; byproducts: (CH3)2NH; (inert atm.); addn. of a soln. of Ph3GeH in acetonitrile to a soln. of Ge amide in acetonitrile, heating at 85°C for 96 h; evapn. in vac., distn. (120°C, 0.05 Torr); elem. anal.;
DOI:10.1021/om900035r

Reference yield: 26.0%

: 23082-96-4
bis(triphenylgermyl)mercury

: 32329-21-8
C₆H₅ClGe

: 53445-88-8
PhMe₂GeGePh₃

: 2817-44-9
methyltriphenylgermane

Guidance literature:: With methyl magnesium iodide; In benzene; to PhGeCl in C6H6 (Ph3Ge)2Hg was added, 12 h at 20°C with stirring, BrCH2CH2Br was added, then MeMgI in ether; hydrolysis, extraction with ether, drying , products were not sepd.; analyzed by cpv;

Reference yield:

: 22702-76-7
phenyldimethylchlorogermane

: 53445-88-8
PhMe₂GeGePh₃

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: acetonitrile

In diethyl ether; acetonitrile;
DOI:10.1021/om900035r