[Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

Base Information

Chemical Name:[Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]
CAS No.:360073-25-2
Molecular Formula:C₂₈H₃₄Au₂NPS₂
Molecular Weight:873.623
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

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Technology Process of [Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

There total 1 articles about [Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 59306-90-0
(N,N-di-n-butyldithiocarbamato)gold(I) dimer

: 321658-49-5
[Au2(μ-C6H3-2-PPh2-5-Me)2]

: 360073-25-2
[Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

Guidance literature:: In dichloromethane; the mixt. of complexes in CH2Cl2 was stirred for 30 min at room temp. (Ar); concd., hexane was added; elem. anal.;
DOI:10.1021/ic010272i

Reference yield: 70.0%

: 360073-25-2
[Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: [AuI(μ-C6H3-2-PPh2-5-Me)AuI(η2-S2CN(n-Bu)2)]

Guidance literature:: In dichloromethane; to a soln. of complex in CH2Cl2 at -70°C was added a soln. of I2 in CH2Cl2, the mixt. was stirred for 30 min, allowed to warm to room temp., stirred for 30 min (Ar); hexane was added, evapd. under reduced pressure, ppt. was filtered, washed with hexane; elem. anal.;
DOI:10.1021/ic010272i

Reference yield: 70.0%

: 360073-25-2
[Au2(μ-C6H3-2-PPh2-5-Me)(μ-S2CN(n-Bu)2)]

: 932-72-9
(Dichloroiodo)benzene

: [AuCl(μ-C6H3-2-PPh2-5-Me)AuCl(η2-S2CN(n-Bu)2)]

Guidance literature:: In dichloromethane; to a soln. of complex in CH2Cl2 at -70°C was added a soln. of C6H5ICl2 in CH2Cl2, the mixt. was stirred for 30 min, allowed to warm to room temp., stirred for 30 min (Ar); hexane was added, evapd. under reduced pressure, ppt. was filtered, washed with hexane; elem. anal.;
DOI:10.1021/ic010272i