[FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)]

Base Information

Chemical Name:[FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)]
CAS No.:435269-17-3
Molecular Formula:C₂₉H₃₁Cl₂FeNP₂
Molecular Weight:582.272
Hs Code.:

[FeCl<sub>2</sub>(bis(2-diphenylphosphinoethyl)methylamine)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)]

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Technology Process of [FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)]

There total 2 articles about [FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: iron(II) chloride

: 686740-94-3
bis[(2-diphenylphosphino)ethyl]methylamine hydrochloride

: 435269-17-3
[FeCl₂(bis(2-diphenylphosphinoethyl)methylamine)]

Guidance literature:: With NaOH; In ethanol; ligand hydrochloride was treated with 10 % NaOH, react. mixt. was extd. with toluene, dried over Na2SO4, solvent was evapd. to dryness, residue was dissolved in EtOH, dropped to soln. FeCl2 in EtOH, stirred at 20°C for 30 min and refluxed for 1 h; soln. was concd. in vacuo and cooled to -5°C, ppt. was filtered off, washed with cold EtOH and dried in vacuo at 60°C, recrystn. from CH2Cl2-petroleum ether; elem. anal.;
DOI:10.1016/S0022-328X(01)01341-9