2,3,4,5-Tetraphenyliodolium Iodide Hydrate

Base Information

• Chemical Name: 2,3,4,5-Tetraphenyliodolium Iodide Hydrate
• CAS No.: 34143-19-6
• Molecular Formula: C₂₈H₂₀I*H₂O*I
• Molecular Weight: 628.291
• Mol file: 34143-19-6.mol

Synonyms:

Chemical Property of 2,3,4,5-Tetraphenyliodolium Iodide Hydrate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,3,4,5-Tetraphenyliodolium Iodide Hydrate

There total 2 articles about 2,3,4,5-Tetraphenyliodolium Iodide Hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

1,1-dimethyl-2,3,4,5-tetraphenylstannole (20195-60-2) → 2,3,4,5-Tetraphenyliodolium Iodide Hydrate (34143-19-6)

Guidance literature:

With iodine trichloride; sodium iodide; In acetone;

DOI:10.1021/jo00333a029

Reference yield:

1,1-dimethyl-2,3,4,5-tetraphenylstannole (20195-60-2) → 2,3,4,5-Tetraphenyliodolium Iodide (34143-19-6)

Guidance literature:

With iodine trichloride; sodium iodide; In acetone;

DOI:10.1021/jo00333a029

Reference yield:

2,3,4,5-Tetraphenyliodolium Iodide Hydrate (34143-19-6) → (Z,Z)-1,4-diiodo-1,2,3,4-tetraphenyl-1,3-butadiene (78479-61-5)

Guidance literature:

at 140 ℃; Thermodynamic data; in CH₂CL₂ solution at room temperature; enthalpy of isomerization;

DOI:10.1021/jo00333a029

upstream raw materials:

1,1-dimethyl-2,3,4,5-tetraphenylstannole

Downstream raw materials:

(Z,Z)-1,4-diiodo-1,2,3,4-tetraphenyl-1,3-butadiene