C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-)

Base Information

• Chemical Name: C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-)
• CAS No.: 1421957-68-7
• Molecular Formula: C₂₇H₂₂O₄P*I
• Molecular Weight: 568.348
• Mol file: 1421957-68-7.mol

Synonyms:

Chemical Property of C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-)

There total 1 articles about C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

caffeic acid (331-39-5,501-16-6) + triphenylphosphine (603-35-0) → C27H22O4P(1+)*I(1-) (1421957-68-7)

Guidance literature:

With iodine; In acetonitrile; for 0.166667h; Inert atmosphere;

DOI:10.1021/jo302502r

Reference yield:

1-Hexadecanol (36653-82-4,124-29-8) + C27H22O4P(1+)*I(1-) (1421957-68-7) → trans-hexadecyl 3-(3,4-dihydroxyphenyl)propenoate

Guidance literature:

C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-); With zinc trifluoromethanesulfonate; In acetonitrile; at 60 ℃; for 3h; Inert atmosphere;

1-Hexadecanol; In acetonitrile; at 60 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jo302502r

Reference yield:

octanol (111-87-5) + C27H22O4P(1+)*I(1-) (1421957-68-7) → (E)-octyl 3-(3,4-dihydroxyphenyl)acrylate

Guidance literature:

C₂₇H₂₂O₄P⁽¹⁺⁾*I^(1-); With zinc trifluoromethanesulfonate; In acetonitrile; at 60 ℃; for 3h; Inert atmosphere;

octanol; In acetonitrile; at 60 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jo302502r

upstream raw materials:

caffeic acid

triphenylphosphine

Downstream raw materials:

(E)-isopropyl 3-(3,4-dihydroxyphenyl)acrylate