(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

Base Information

Chemical Name:(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol
CAS No.:131685-51-3
Molecular Formula:C₁₅H₂₄O₃
Molecular Weight:252.354
Hs Code.:

Synonyms:

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Chemical Property of (R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

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Technology Process of (R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

There total 4 articles about (R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131725-09-2
(R)-(+)-2-ethylpent-4-enoic acid

: 131685-51-3
(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 4 h / Ambient temperature

2: 1) sodium hydride (60percent in oil) / 1) THF, DMF 0 deg C, 15 min, 2) r.t., 20 h

3: 1) 9-borabicyclo<3.3.1>nonane, 2) NaOH / 1) THF, r.t., 30 min, 2) H₂O, r.t., 3 h

With sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; sodium hydride; In diethyl ether;
DOI:10.1021/jo00313a011

Reference yield:

: 130710-56-4
(S)-3-<(R)-2-ethyl-1-oxo-4-penten-1-yl>-4-(phenylmethyl)-1,3-oxazolidin-2-one

: 131685-51-3
(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

Guidance literature:: Multi-step reaction with 4 steps

1: 30percent aq. H₂O₂, LiOH, H₂O / tetrahydrofuran / 1 h / 0 °C

2: LiAlH₄ / diethyl ether / 4 h / Ambient temperature

3: 1) sodium hydride (60percent in oil) / 1) THF, DMF 0 deg C, 15 min, 2) r.t., 20 h

4: 1) 9-borabicyclo<3.3.1>nonane, 2) NaOH / 1) THF, r.t., 30 min, 2) H₂O, r.t., 3 h

With lithium hydroxide; sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; water; dihydrogen peroxide; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00313a011

Reference yield:

: 131685-50-2
(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexene

: 131685-51-3
(R)-4-<<(4-methoxyphenyl)methoxy>methyl>-1-hexanol

Guidance literature:: With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; Yield given. Multistep reaction; 1) THF, r.t., 30 min, 2) H₂O, r.t., 3 h;
DOI:10.1021/jo00313a011