MeO(C₆H₄)CH₂N(SiMe₂Ph)2

Base Information

• Chemical Name: MeO(C₆H₄)CH₂N(SiMe₂Ph)2
• CAS No.: 1258944-85-2
• Molecular Formula: C₂₄H₃₁NOSi₂
• Molecular Weight: 405.687

Synonyms:

Chemical Property of MeO(C₆H₄)CH₂N(SiMe₂Ph)2

Chemical Property:

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Technology Process of MeO(C₆H₄)CH₂N(SiMe₂Ph)2

There total 1 articles about MeO(C₆H₄)CH₂N(SiMe₂Ph)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dimethylphenylsilane (766-77-8) + 4-methoxybenzonitrile (874-90-8) → MeO(C6H4)CH2N(SiMe2Ph)2 (1258944-85-2)

Guidance literature:

With CpRu(PiPr₃)(CH₃CN)2BAR; In dichloromethane-d2; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201003069

Reference yield:

MeO(C6H4)CH2N(SiMe2Ph)2 (1258944-85-2) → 4-methoxybenzylamine hydrochloride (17061-61-9)

Guidance literature:

With hydrogenchloride; water; In diethyl ether; at 20 ℃; for 1h;

DOI:10.1021/acs.joc.5b00941

upstream raw materials:

Dimethylphenylsilane

4-methoxybenzonitrile

Downstream raw materials:

4-methoxybenzylamine hydrochloride

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