trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure

Base Information

• Chemical Name: trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure
• CAS No.: 14378-07-5
• Molecular Formula: C₁₀H₆ClNO₂
• Molecular Weight: 207.616
• Mol file: 14378-07-5.mol

Synonyms:

Chemical Property of trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure

There total 2 articles about trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyanoacetic acid (372-09-8) + m-Chlorobenzaldehyde (587-04-2) → trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure (14378-07-5,91799-74-5)

Guidance literature:

With sodium hydroxide; sodium carbonate; for 1h;

DOI:10.1021/jm980566m

Reference yield:

→ trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure (14378-07-5,91799-74-5)

Guidance literature:

3-Chlor-benzaldehyd, Cyanessigsaeure-aethylester / Eg. + Perchlorsaeure bei 25grad;

DOI:10.1039/jr9620000731

Reference yield:

trans-2-<3-Chlor-benzyliden>-2-cyan-essigsaeure (14378-07-5,91799-74-5) → (3-chlorophenyl)acrylonitrile (14378-03-1,81020-60-2,24654-47-5)

Guidance literature:

With copper(I) oxide; under 0.5 Torr; Heating;

DOI:10.1021/jm980566m

upstream raw materials:

cyanoacetic acid

m-Chlorobenzaldehyde

Downstream raw materials:

(3-chlorophenyl)acrylonitrile