3-amino-4-oxo-4-phenylbutyric acid hydrobromide

Base Information

Chemical Name:3-amino-4-oxo-4-phenylbutyric acid hydrobromide
CAS No.:112160-47-1
Molecular Formula:BrH*C₁₀H₁₁NO₃
Molecular Weight:274.114
Hs Code.:

Synonyms:

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Chemical Property of 3-amino-4-oxo-4-phenylbutyric acid hydrobromide

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Technology Process of 3-amino-4-oxo-4-phenylbutyric acid hydrobromide

There total 3 articles about 3-amino-4-oxo-4-phenylbutyric acid hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 112160-47-1
3-amino-4-oxo-4-phenylbutyric acid hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 2 h / Ambient temperature

2: formic acid / 3 h / 40 - 50 °C

3: 1.) 33percent HBr / 1.) acetic acid, r.t; 2.) 50 deg C, 3 h

With formic acid; hydrogen bromide; triethylamine; In tetrahydrofuran;
DOI:10.1248/cpb.34.4516

Reference yield:

: 112160-48-2
dibenzyl α-benzoyl-α-formylaminosuccinate

: 112160-47-1
3-amino-4-oxo-4-phenylbutyric acid hydrobromide

Guidance literature:: With hydrogen bromide; Yield given. Multistep reaction; 1.) acetic acid, r.t; 2.) 50 deg C, 3 h;
DOI:10.1248/cpb.34.4516

Reference yield:

: 112160-49-3
2-Benzoyl-2-isocyano-succinic acid dibenzyl ester

: 112160-47-1
3-amino-4-oxo-4-phenylbutyric acid hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / 3 h / 40 - 50 °C

2: 1.) 33percent HBr / 1.) acetic acid, r.t; 2.) 50 deg C, 3 h

With formic acid; hydrogen bromide;
DOI:10.1248/cpb.34.4516