C₆₅H₇₆O₉Si

Base Information

Chemical Name:C₆₅H₇₆O₉Si
CAS No.:115030-99-4
Molecular Formula:C₆₅H₇₆O₉Si
Molecular Weight:1029.4
Hs Code.:

C<sub>65</sub>H<sub>76</sub>O<sub>9</sub>Si

Synonyms:

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Chemical Property of C₆₅H₇₆O₉Si

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Technology Process of C₆₅H₇₆O₉Si

There total 6 articles about C₆₅H₇₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 115030-99-4,115114-84-6
C₆₅H₇₆O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium tosylate / benzene / 2 h / 80 °C

2: !) nBuLi; 2) PhSeCl; 3) 3-chloroperoxybenzoic acid, aq. NaHCO₃ / 1) THF, -78 deg C, 30 min; 2) THF, -78 deg C, 15 min; 3) THF, 10 deg C, 20 min

3: 1) tBuLi; 3) Na-Hg, Na₂HPO₄ / 1) THF, -78 deg C, 20 min; 2) THF, -78 deg C to room temp.; 3) MeOH, THF, -30 deg C, 30 min

With disodium hydrogenphosphate; sodium amalgam; tert.-butyl lithium; pyridinium p-toluenesulfonate; In benzene;
DOI:10.1016/S0040-4039(00)96835-7

Reference yield:

: 115030-95-0,115075-71-3,127854-64-2,127854-65-3
(1R,3S,4S,6S)-1-((S)-3-Benzenesulfonyl-1-hydroxymethyl-propyl)-6-(tert-butyl-diphenyl-silanyloxymethyl)-4-methyl-cyclohexane-1,3-diol

: 115030-99-4,115114-84-6
C₆₅H₇₆O₉Si

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium tosylate / benzene / 2 h / 80 °C

2: !) nBuLi; 2) PhSeCl; 3) 3-chloroperoxybenzoic acid, aq. NaHCO₃ / 1) THF, -78 deg C, 30 min; 2) THF, -78 deg C, 15 min; 3) THF, 10 deg C, 20 min

3: 1) tBuLi; 3) Na-Hg, Na₂HPO₄ / 1) THF, -78 deg C, 20 min; 2) THF, -78 deg C to room temp.; 3) MeOH, THF, -30 deg C, 30 min

With disodium hydrogenphosphate; sodium amalgam; tert.-butyl lithium; pyridinium p-toluenesulfonate; In benzene;
DOI:10.1016/S0040-4039(00)96835-7

Reference yield:

: 115075-76-8
(+)-(1S,3S,4S,6S)-6-<(tert-butyldiphenylsilyloxy)methyl>-4-methyl-1-<1-methylene-3-(phenylsulphonyl)propyl>-1,3-cyclohexanediol

: 115030-99-4,115114-84-6
C₆₅H₇₆O₉Si

Guidance literature:: Multi-step reaction with 4 steps

1: 1) BH₃*Me₂S; 2) NaOH, aq. H₂O₂ / 1) THF, -20 deg C, 16 h; 2) H₂O, room temp., 30 min

2: pyridinium tosylate / benzene / 2 h / 80 °C

3: !) nBuLi; 2) PhSeCl; 3) 3-chloroperoxybenzoic acid, aq. NaHCO₃ / 1) THF, -78 deg C, 30 min; 2) THF, -78 deg C, 15 min; 3) THF, 10 deg C, 20 min

4: 1) tBuLi; 3) Na-Hg, Na₂HPO₄ / 1) THF, -78 deg C, 20 min; 2) THF, -78 deg C to room temp.; 3) MeOH, THF, -30 deg C, 30 min

With sodium hydroxide; disodium hydrogenphosphate; sodium amalgam; dimethylsulfide borane complex; dihydrogen peroxide; tert.-butyl lithium; pyridinium p-toluenesulfonate; In benzene;
DOI:10.1016/S0040-4039(00)96835-7