C₅₂H₅₄N₂O₅

Base Information

• Chemical Name: C₅₂H₅₄N₂O₅
• CAS No.: 1354328-18-9
• Molecular Formula: C₅₂H₅₄N₂O₅
• Molecular Weight: 787.011
• Mol file: 1354328-18-9.mol

Synonyms:

Chemical Property of C₅₂H₅₄N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₂H₅₄N₂O₅

There total 10 articles about C₅₂H₅₄N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

→ C52H54N2O5 (1354328-18-9)

Guidance literature:

In methanol; at 20 ℃; for 3h;

Reference yield:

C20H26N2O3 → C52H54N2O5 (1354328-18-9)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

2: methanol / 3 h / 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; In methanol;

DOI:10.1021/ml200278u

Reference yield:

1-Bromopentane (110-53-2) → C52H54N2O5 (1354328-18-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: formic acid; sodium cyanoborohydride / methanol / 6 h / 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / methanol / 3 h / 20 °C

4.1: methanol / 3 h / 20 °C / Inert atmosphere

With formic acid; palladium on activated charcoal; hydrogen; sodium hydride; sodium cyanoborohydride; In methanol; N,N-dimethyl-formamide; mineral oil;

DOI:10.1021/ml200278u

upstream raw materials:

C₄₀H₃₆O₅

1-Bromopentane

trityl chloride

4-hydroxy-benzaldehyde

Downstream raw materials:

C₆₇H₇₃N₅O₉