(1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

Base Information

Chemical Name:(1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid
CAS No.:74830-56-1
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:

Synonyms:

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Chemical Property of (1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

Chemical Property:

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Technology Process of (1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

There total 5 articles about (1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: (1SR,2RS)-ethyl 2-cyclohexylcyclopropanecarboxylate

: 74830-56-1,74830-57-2,91056-79-0
(1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃; for 18h;
DOI:10.1021/jacs.5b05215

Reference yield:

: 695-12-5,25498-06-0
vinylcyclohexane

: 74830-56-1,74830-57-2,91056-79-0
(1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: CuSO₄

2: (alkaline hydrolysis)

With copper(II) sulfate;

Reference yield:

: 6048-09-5
3-cyclohexylacrylic acid ethyl ester

: 74830-56-1,74830-57-2,91056-79-0
(1SR,2RS)-2-cyclohexylcyclopropanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethyl sulfoxide / 50 °C

2: sodium hydroxide / methanol / 50 °C

With sodium hydride; sodium hydroxide; In methanol; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.09.069