C₁₈H₂₈N₄Si

Base Information

Chemical Name:C₁₈H₂₈N₄Si
CAS No.:1415918-96-5
Molecular Formula:C₁₈H₂₈N₄Si
Molecular Weight:328.533
Hs Code.:

C<sub>18</sub>H<sub>28</sub>N<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₈N₄Si

Chemical Property:

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Technology Process of C₁₈H₂₈N₄Si

There total 1 articles about C₁₈H₂₈N₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21692-54-6
triethyl(cyclohex-1-en-1-ylethynyl)silane

: 214907-09-2
4,6-diamino-5-iodopyrimidine

: 1415918-96-5
C₁₈H₂₈N₄Si

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; lithium chloride; In N,N-dimethyl-formamide; at 95 ℃; regioselective reaction;
DOI:10.1016/j.bmcl.2012.08.020

Reference yield:

: 1415918-96-5
C₁₈H₂₈N₄Si

: C₁₇H₂₁IN₄O

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; dmap / N,N-dimethyl-formamide

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 50 °C

3: N-iodo-succinimide / N,N-dimethyl-formamide / 20 - 45 °C

With dmap; N-iodo-succinimide; lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.08.020

Reference yield:

: 1415918-96-5
C₁₈H₂₈N₄Si

: 1403893-82-2
C₂₇H₃₅N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; dmap / N,N-dimethyl-formamide

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 50 °C

3: N-iodo-succinimide / N,N-dimethyl-formamide / 20 - 45 °C

4: lithium chloride; sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; ethanol; water / 80 °C

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-iodo-succinimide; lithium aluminium tetrahydride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium chloride; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene; 4: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.020