6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

Base Information

Chemical Name:6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid
CAS No.:244055-05-8
Molecular Formula:C₁₆H₂₄N₂O₄
Molecular Weight:308.378
Hs Code.:

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Chemical Property of 6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

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Technology Process of 6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

There total 3 articles about 6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 244055-04-7
6-(n-propylamino)hexanoic acid

: 244055-05-8
6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

Guidance literature:: With triethylamine; In methanol; for 48h;
DOI:10.1016/S0968-0896(99)00026-7

Reference yield:

: 372-52-1
6-amino-n-caproic acid n-hexyl ester

: 244055-05-8
6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 16 percent / NaBH₃CN / acetic acid; methanol / 48 h / 20 °C

2: 94 percent / aq. NaOH / methanol / 1 h

3: 22 percent / Et₃N / methanol / 48 h

With sodium hydroxide; sodium cyanoborohydride; triethylamine; In methanol; acetic acid; 1: Addition / 2: Hydrolysis / 3: Alkylation;
DOI:10.1016/S0968-0896(99)00026-7

Reference yield:

: 244055-03-6
6-N-propylamino caproic acid n-hexyl ester

: 244055-05-8
6-[N-(4-nitrobenzyl)-N-propyl]-amino caproic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / methanol / 1 h

2: 22 percent / Et₃N / methanol / 48 h

With sodium hydroxide; triethylamine; In methanol; 1: Hydrolysis / 2: Alkylation;
DOI:10.1016/S0968-0896(99)00026-7