Technology Process of Benzamide, 2-chloro-4-methoxy-6-nitro-N-phenyl-
There total 3 articles about Benzamide, 2-chloro-4-methoxy-6-nitro-N-phenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) NaNO2, conc. H2SO4, 2) Na2CO3 / 1) acetic acid, room temperature, 2) H2O, room temperature, 3 h
2: 78 percent / conc. H2SO4, NaNO2 / acetic acid; H2O / a) 140 deg C, b) 100 deg C, 30 min
3: SOCl2 / 1 h / Heating
4: benzene / 2 h / Ambient temperature
With
thionyl chloride; sulfuric acid; sodium carbonate; sodium nitrite;
In
water; acetic acid; benzene;
DOI:10.1248/cpb.39.2400
- Guidance literature:
-
Multi-step reaction with 2 steps
1: SOCl2 / 1 h / Heating
2: benzene / 2 h / Ambient temperature
With
thionyl chloride;
In
benzene;
DOI:10.1248/cpb.39.2400
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 25 percent / sulfuryl chloride / acetic acid / 0.5 h / Ambient temperature
2: 1) NaNO2, conc. H2SO4, 2) Na2CO3 / 1) acetic acid, room temperature, 2) H2O, room temperature, 3 h
3: 78 percent / conc. H2SO4, NaNO2 / acetic acid; H2O / a) 140 deg C, b) 100 deg C, 30 min
4: SOCl2 / 1 h / Heating
5: benzene / 2 h / Ambient temperature
With
thionyl chloride; sulfuryl dichloride; sulfuric acid; sodium carbonate; sodium nitrite;
In
water; acetic acid; benzene;
DOI:10.1248/cpb.39.2400
