2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide

Base Information

Chemical Name:2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide
CAS No.:145291-87-8
Molecular Formula:C₁₅H₉IO₂
Molecular Weight:348.14
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide

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Technology Process of 2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide

There total 6 articles about 2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.8%

: I-phenyl-I-(4'-benzoyl-2-iodobenzoyl)iodonium ylide

: 145291-87-8,152151-76-3
2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide

Guidance literature:: With copper acetylacetonate; In benzene; for 1h; Reflux;
DOI:10.24820/ARK.5550190.P011.667

Reference yield:

: 145291-94-7
1-(2-iodophenyl)-3-phenylpropane-1,3-dione

: 145291-87-8,152151-76-3
2-benzoyl-3-oxo-2,3-dihydrobenzo[b]iodolyl ylide

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol / 0 °C

2: Cu(acac)2 (Hacac = pentane-2,4-dione) / benzene / 1 h / Heating

With copper acetylacetonate; potassium hydroxide; In methanol; benzene;
DOI:10.1039/c39920001487