4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

Base Information

Chemical Name:4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone
CAS No.:116693-22-2
Molecular Formula:C₂₅H₂₅Cl₆N₃O₆
Molecular Weight:676.208
Hs Code.:

4-(2,2,2-trichloroethoxycarbonylamino)-2-<N-(2,2,2-trichloroethoxycarbonyl)<hydroxy(p-toluidino)methyl>amino>but-3-enyl phenyl ketone

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Chemical Property of 4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

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Technology Process of 4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

There total 2 articles about 4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109853-26-1
2-hydroxy-4-phenacyl-1,2,3,4-tetrahydropyrimidine

: 116693-22-2
4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; ethyl acetate / 19 h / Ambient temperature

2: 1.) MgSO₄, trifluoroacetic acid (TFA) / 1.) CH₂Cl₂, 10 min; 2.) CH₂Cl₂, reflux, 23 h

With magnesium sulfate; trifluoroacetic acid; In pyridine; ethyl acetate;
DOI:10.1039/P19880000725

Reference yield:

: 109853-28-3
8,9-bis-(2,2,2-trichloroethoxycarbonyl)-3-phenyl-2-oxa-8,9-diazabicyclo<3.3.1>nona-3,6-diene

: 106-49-0,12221-03-3
p-toluidine

: 116693-20-0
3-phenyl-2-(p-tolyl)-8,9-bis-(2,2,2-trichloroethoxycarbonyl)-2,8,9-triazabicyclo<3.3.1>nona-3,6-diene

: 116693-22-2
4-(2,2,2-trichloroethoxycarbonylamino)-2-amino>but-3-enyl phenyl ketone

Guidance literature:: With magnesium sulfate; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 10 min; 2.) CH₂Cl₂, reflux, 23 h;
DOI:10.1039/P19880000725