L-phenylalanyl-L-phenylalanine dimethylamide

Base Information

Chemical Name:L-phenylalanyl-L-phenylalanine dimethylamide
CAS No.:96574-62-8
Molecular Formula:C₂₀H₂₅N₃O₂
Molecular Weight:339.437
Hs Code.:

Synonyms:

Suppliers and Price of L-phenylalanyl-L-phenylalanine dimethylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of L-phenylalanyl-L-phenylalanine dimethylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of L-phenylalanyl-L-phenylalanine dimethylamide

There total 3 articles about L-phenylalanyl-L-phenylalanine dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Boc-Phe-Phe-N(CH₃)2

: 96574-62-8
L-phenylalanyl-L-phenylalanine dimethylamide

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.bmc.2008.05.001

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 96574-62-8
L-phenylalanyl-L-phenylalanine dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1.) DCC, 2.) 33percent HBr / 1.) CH₂Cl₂, r.t., 2 h, 2.) AcOH, 0 deg C, 3 h

2: 1.) DCC, (i-pr)2EtN, 2.) H₂ / 2.) 5percent Pd/C / 1.) CH₂Cl₂, 0 deg C, 30 min., r.t., 6 h, 2.) EtOH, AcOH, r.t., 8 h

With hydrogen bromide; hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal;
DOI:10.1002/hlca.19920750522

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 104347-81-1
L-Phenylalanine Dimethylamide Hydrobromide

: 96574-62-8
L-phenylalanyl-L-phenylalanine dimethylamide

Guidance literature:: With hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; Yield given. Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 30 min., r.t., 6 h, 2.) EtOH, AcOH, r.t., 8 h;
DOI:10.1002/hlca.19920750522