cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)

Base Information

Chemical Name:cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)
CAS No.:258884-20-7
Molecular Formula:C₉₆H₁₀₀Cl₂O₆P₄Pt
Molecular Weight:1739.73
Hs Code.:

cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)

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Chemical Property of cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)

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Technology Process of cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)

There total 1 articles about cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 124-43-6
urea hydrogen peroxide adduct

: 172036-64-5
cone-5,11,17,23-tetra-tert-butyl-25,26,27,28-tetrakis(diphenylphosphinomethoxy)calix[4]arene

: 258884-20-7
cis-dichloro(5,11,17,23-tetra-tert-butyl-25,26-bis(diphenylphosphinoylmethoxy)-27,28-bis(diphenylphosphinomethoxy)calix[4]arene-P,P')platinum(II)

Guidance literature:: In tetrahydrofuran; addn. of Pt complex in THF to ligand in THF, stirring (1 h), addn. of H2O2-urea adduct, further vigorous stirring (1 h); filtration, evapn. to dryness, flash chromy. (SiO2; EtOAc/hexane); elem.anal.;
DOI:10.1039/a905814a