C₁₃⁽¹³⁾CH₁₀BrF

Base Information

• Chemical Name: C₁₃⁽¹³⁾CH₁₀BrF
• CAS No.: 193673-34-6
• Molecular Formula: C₁₄H₁₀BrF
• Molecular Weight: 278.125
• Mol file: 193673-34-6.mol

Synonyms:

Chemical Property of C₁₃⁽¹³⁾CH₁₀BrF

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃⁽¹³⁾CH₁₀BrF

There total 4 articles about C₁₃⁽¹³⁾CH₁₀BrF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) → C13(13)CH10BrF (193673-34-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 38 percent / HMDS-Li / tetrahydrofuran; hexamethylphosphoric acid triamide / -110 °C

2: 98 percent / TsOH / toluene / 48 h / Heating

3: 89 percent / NaOH / dioxane / 24 h / Ambient temperature

4: 1.) Br₂; 2.) Na₂SO₃ / 1.) CHCl₃, 32 h, reflux; 2.) H₂O, 48 h, rt

With sodium hydroxide; bromine; toluene-4-sulfonic acid; lithium hexamethyldisilazane; sodium sulfite; In tetrahydrofuran; 1,4-dioxane; N,N,N,N,N,N-hexamethylphosphoric triamide; toluene;

DOI:10.1016/S0040-4039(97)01017-4

Reference yield:

C16(13)CH15FO2 (193673-30-2) → C13(13)CH10BrF (193673-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / NaOH / dioxane / 24 h / Ambient temperature

2: 1.) Br₂; 2.) Na₂SO₃ / 1.) CHCl₃, 32 h, reflux; 2.) H₂O, 48 h, rt

With sodium hydroxide; bromine; sodium sulfite; In 1,4-dioxane;

DOI:10.1016/S0040-4039(97)01017-4

Reference yield:

C16(13)CH17FO3 (193673-28-8) → C13(13)CH10BrF (193673-34-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 98 percent / TsOH / toluene / 48 h / Heating

2: 89 percent / NaOH / dioxane / 24 h / Ambient temperature

3: 1.) Br₂; 2.) Na₂SO₃ / 1.) CHCl₃, 32 h, reflux; 2.) H₂O, 48 h, rt

With sodium hydroxide; bromine; toluene-4-sulfonic acid; sodium sulfite; In 1,4-dioxane; toluene;

DOI:10.1016/S0040-4039(97)01017-4

upstream raw materials:

C₁₄⁽¹³⁾CH₁₁FO₂

benzophenone

C₁₆⁽¹³⁾CH₁₅FO₂

C₁₆⁽¹³⁾CH₁₇FO₃