C₃₁H₅₁F₇NO₆P

Base Information

Chemical Name:C₃₁H₅₁F₇NO₆P
CAS No.:108330-88-7
Molecular Formula:C₃₁H₅₁F₇NO₆P
Molecular Weight:697.712
Hs Code.:

C<sub>31</sub>H<sub>51</sub>F<sub>7</sub>NO<sub>6</sub>P

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₅₁F₇NO₆P

Chemical Property:

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Technology Process of C₃₁H₅₁F₇NO₆P

There total 13 articles about C₃₁H₅₁F₇NO₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50816-18-7
9-decen-1-yl acetate

: 108330-88-7
C₃₁H₅₁F₇NO₆P

Guidance literature:: Multi-step reaction with 13 steps

1: Fe₃(CO)12 / 5.5 h / 80 °C

2: Zn powder / acetic acid; diethyl ether / 1 h / Ambient temperature

3: 5 percent methanolic KOH / 2 h / Ambient temperature

4: 85 percent / triphenylphosphine dibromide / dimethylformamide; acetonitrile

5: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

6: 80 percent / H₂ / 5 percent Pd-C / ethanol; acetic acid / Ambient temperature

7: 87 percent / pyridine / 1 h / Ambient temperature

8: 75 percent / 22 percent KH / benzene; paraffin / 1.) 30 min; 2.) 10 h, RT

9: 77 percent / 2 N HCl / tetrahydrofuran / 2 h / Ambient temperature

10: Pb(OAc)4 / benzene / 1 h

11: NaBH₄ / methanol / Ambient temperature

12: triethylamine / diethyl ether / 1.) 12 h, reflux; 2.) 1 h, reflux

13: 2.) AgOAc / 1.) methanol, 55 deg C, 12 h; 2.) aq. methanol, 2 h

With lead(IV) acetate; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; hydrogen; silver(I) acetate; potassium hydride; triethylamine; zinc; dibromotriphenylphosphorane; palladium on activated charcoal; dilithium tetrachlorocuprate; triiron dodecarbonyl; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; acetic acid; N,N-dimethyl-formamide; acetonitrile; paraffin; benzene;
DOI:10.1248/cpb.35.647

Reference yield:

: 102197-76-2
1-bromo-11,11,12,12,13,13,13-heptafluorotridecane

: 108330-88-7
C₃₁H₅₁F₇NO₆P

Guidance literature:: Multi-step reaction with 9 steps

1: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

2: 80 percent / H₂ / 5 percent Pd-C / ethanol; acetic acid / Ambient temperature

3: 87 percent / pyridine / 1 h / Ambient temperature

4: 75 percent / 22 percent KH / benzene; paraffin / 1.) 30 min; 2.) 10 h, RT

5: 77 percent / 2 N HCl / tetrahydrofuran / 2 h / Ambient temperature

6: Pb(OAc)4 / benzene / 1 h

7: NaBH₄ / methanol / Ambient temperature

8: triethylamine / diethyl ether / 1.) 12 h, reflux; 2.) 1 h, reflux

9: 2.) AgOAc / 1.) methanol, 55 deg C, 12 h; 2.) aq. methanol, 2 h

With lead(IV) acetate; hydrogenchloride; sodium tetrahydroborate; hydrogen; silver(I) acetate; potassium hydride; triethylamine; palladium on activated charcoal; dilithium tetrachlorocuprate; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; acetic acid; paraffin; benzene;
DOI:10.1248/cpb.35.647

Reference yield:

: 102197-75-1
11,11,12,12,13,13,13-heptafluorotridecan-1-ol

: 108330-88-7
C₃₁H₅₁F₇NO₆P

Guidance literature:: Multi-step reaction with 10 steps

1: 85 percent / triphenylphosphine dibromide / dimethylformamide; acetonitrile

2: 40 percent / 0.1 M Li₂CuCl₄ / tetrahydrofuran / 5 h / Ambient temperature

3: 80 percent / H₂ / 5 percent Pd-C / ethanol; acetic acid / Ambient temperature

4: 87 percent / pyridine / 1 h / Ambient temperature

5: 75 percent / 22 percent KH / benzene; paraffin / 1.) 30 min; 2.) 10 h, RT

6: 77 percent / 2 N HCl / tetrahydrofuran / 2 h / Ambient temperature

7: Pb(OAc)4 / benzene / 1 h

8: NaBH₄ / methanol / Ambient temperature

9: triethylamine / diethyl ether / 1.) 12 h, reflux; 2.) 1 h, reflux

10: 2.) AgOAc / 1.) methanol, 55 deg C, 12 h; 2.) aq. methanol, 2 h

With lead(IV) acetate; hydrogenchloride; sodium tetrahydroborate; hydrogen; silver(I) acetate; potassium hydride; triethylamine; dibromotriphenylphosphorane; palladium on activated charcoal; dilithium tetrachlorocuprate; In tetrahydrofuran; pyridine; methanol; diethyl ether; ethanol; acetic acid; N,N-dimethyl-formamide; acetonitrile; paraffin; benzene;
DOI:10.1248/cpb.35.647