Diethylmesitylphosphinoxid

Base Information

• Chemical Name: Diethylmesitylphosphinoxid
• CAS No.: 29634-10-4
• Molecular Formula: C₁₃H₂₁OP
• Molecular Weight: 224.283
• Mol file: 29634-10-4.mol

Synonyms:

Chemical Property of Diethylmesitylphosphinoxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diethylmesitylphosphinoxid

There total 6 articles about Diethylmesitylphosphinoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

mesityldivinylphosphine oxide + potassium 4-(methoxy)phenyltrifluoroborate → Diethylmesitylphosphinoxid (29634-10-4) + C20H23O2P + C13H19OP + C27H29O3P + C20H25O2P + C20H25O2P + C20H25O2P

Guidance literature:

With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; potassium phosphate; (RhCl(diene*))₂; In water; toluene; at 80 ℃; for 14h; enantioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201712572

Reference yield:

mesityldivinylphosphine oxide + potassium 4-(methoxy)phenyltrifluoroborate → Diethylmesitylphosphinoxid (29634-10-4) + C20H23O2P + C13H19OP + C27H29O3P + C20H27O2P + C20H25O2P + C20H25O2P + C20H25O2P

Guidance literature:

With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; potassium phosphate; [RhCl(cis-cyclooctene)2]2; In 1,4-dioxane; water; at 80 ℃; for 14h; enantioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201712572

Reference yield:

→ Diethylmesitylphosphinoxid (29634-10-4)

Guidance literature:

Diethylmesitylphosphin, H2O2;

upstream raw materials:

dichloro(mesityl)phosphane

2-mesitylmagnesium bromide