dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate

Base Information

Chemical Name:dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate
CAS No.:714960-49-3
Molecular Formula:BF₄*C₂₅H₁₉FeO₄
Molecular Weight:526.075
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate

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Technology Process of dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate

There total 1 articles about dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 76391-69-0
Fp-FBF₃

: 922-67-8
propynoic acid methyl ester

: 501-65-5
diphenyl acetylene

: 714960-49-3
dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate

Guidance literature:: In dichloromethane; (Ar); methyl propiolate was added via syringe to soln. of Fe complex in CH2Cl2; mixt. was stirred for 30 min; alkyne was added; soln. was stirred overnight; filtered through Celite; solvent removed (vac.); THF transferred (vac.) to residue; concd. (vac.); cooled to -30°C overnight; isolated byfilter cannulation; washed (Et2O); elem. anal.;
DOI:10.1021/om0343420