(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

Base Information

Chemical Name:(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester
CAS No.:192884-02-9
Molecular Formula:C₂₉H₃₂N₄O₆S₂
Molecular Weight:596.728
Hs Code.:

(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

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Chemical Property of (4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

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Technology Process of (4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

There total 1 articles about (4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93711-81-0,90776-59-3,189188-38-3
(4-nitrophenyl)methyl (4R,5R,6S)-3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

: 4-Benzyl-piperazine-1-carbodithioic acid; compound with triethyl-amine

: 192884-02-9
(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

Guidance literature:: With lithium chloride; In tetrahydrofuran; Ambient temperature;
DOI:10.1016/S0960-894X(97)00272-2

Reference yield:

: 192884-02-9
(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

: 74-88-4
methyl iodide

: C₂₃H₂₉N₃O₄S₂

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; Multistep reaction; 1.) THF, acetone, 0 deg C, 2 h; room temperature, 2 h, 2.) THF, EtOH, room temperature, overnight;
DOI:10.1016/S0968-0896(98)00069-8

Reference yield:

: 192884-02-9
(4R,5S,6S)-3-(4-Benzyl-piperazine-1-carbothioylsulfanyl)-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-ene-2-carboxylic acid 4-nitro-benzyl ester

: 74-88-4
methyl iodide

: 1-Benzyl-4-[(4R,5S,6S)-2-carboxy-6-((R)-1-hydroxy-ethyl)-4-methyl-7-oxo-1-aza-bicyclo[3.2.0]hept-2-en-3-ylsulfanylthiocarbonyl]-1-methyl-piperazin-1-ium; iodide

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; Multistep reaction; 1.) THF, room temperature, 2.) THF, H₂O, room temperature;
DOI:10.1016/S0960-894X(97)00272-2