Technology Process of C61H80N8O13Si
There total 11 articles about C61H80N8O13Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) -78 deg C, 2.) -78 deg C
3: 90 percent / Ph3P, H2O / tetrahydrofuran
4: 60 percent / NaCNBH3 / ethanol / pH 5,5
5: H2 / Pd-C / methanol
6: i-Bu2AlH
7: NaCNBH3 / ethanol / pH 5,5
With
oxalyl dichloride; water; hydrogen; diisobutylaluminium hydride; sodium cyanoborohydride; dimethyl sulfoxide; triethylamine; triphenylphosphine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.1016/S0040-4039(00)61716-1
- Guidance literature:
-
Multi-step reaction with 9 steps
1: ZnBr2 / nitromethane / 6 h / 0 °C
2: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) -78 deg C, 2.) -78 deg C
4: H2 / Pd-C
5: i-Bu2AlH / -78 °C
6: 60 percent / NaCNBH3 / ethanol / pH 5,5
7: H2 / Pd-C / methanol
8: i-Bu2AlH
9: NaCNBH3 / ethanol / pH 5,5
With
oxalyl dichloride; hydrogen; diisobutylaluminium hydride; sodium cyanoborohydride; dimethyl sulfoxide; triethylamine; zinc dibromide;
palladium on activated charcoal;
In
methanol; nitromethane; ethanol;
DOI:10.1016/S0040-4039(00)61716-1
- Guidance literature:
-
Multi-step reaction with 6 steps
2: 90 percent / Ph3P, H2O / tetrahydrofuran
3: 60 percent / NaCNBH3 / ethanol / pH 5,5
4: H2 / Pd-C / methanol
5: i-Bu2AlH
6: NaCNBH3 / ethanol / pH 5,5
With
water; hydrogen; diisobutylaluminium hydride; sodium cyanoborohydride; triphenylphosphine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.1016/S0040-4039(00)61716-1
