1-BOC-3-ALLYLPIPERIDIN-4-ONE

Base Information

Chemical Name:1-BOC-3-ALLYLPIPERIDIN-4-ONE
CAS No.:138021-97-3
Molecular Formula:C13H21NO3
Molecular Weight:239.31100
Hs Code.:
Mol file:138021-97-3.mol

Synonyms:N-(t-BOC)-3-allyl-4-piperidone;4-oxo-3-(2-propenyl)-1-piperidinecarboxylic acid, 1,1-dimethylethyl ester;tert-butyl 3-allyl-4-oxopiperidine-1-carboxylate;(3RS)-3-allyl-4-oxopiperidine-1-carboxylic acid tert-butyl ester;

Suppliers and Price of 1-BOC-3-ALLYLPIPERIDIN-4-ONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-butyl3-allyl-4-oxopiperidine-1-carboxylate
100mg
$ 220.00

Crysdot
tert-Butyl3-allyl-4-oxopiperidine-1-carboxylate 95%
1g
$ 450.00

Crysdot
tert-Butyl3-allyl-4-oxopiperidine-1-carboxylate 95%
250mg
$ 180.00

Alichem
tert-Butyl3-allyl-4-oxopiperidine-1-carboxylate
1g
$ 499.50

Alichem
tert-Butyl3-allyl-4-oxopiperidine-1-carboxylate
250mg
$ 196.20

Total 2 raw suppliers

Chemical Property of 1-BOC-3-ALLYLPIPERIDIN-4-ONE

Chemical Property:

PSA：46.61000
LogP:2.32650

Purity/Quality:

99% ^*data from raw suppliers

tert-butyl3-allyl-4-oxopiperidine-1-carboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-BOC-3-ALLYLPIPERIDIN-4-ONE

There total 5 articles about 1-BOC-3-ALLYLPIPERIDIN-4-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 107-18-6
allyl alcohol

: 138021-97-3
tert-butyl 3-allyl-4-oxopiperidine-1-carboxylate

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); toluene-4-sulfonic acid; 2,2-dimethoxy-propane; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; rac-Pro-OH; In dimethyl sulfoxide; at 70 ℃;
DOI:10.1002/chem.201503653

Reference yield: 24.0%

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 106-95-6
allyl bromide

: 138021-97-3
tert-butyl 3-allyl-4-oxopiperidine-1-carboxylate

Guidance literature:: N-tert-butyloxycarbonylpiperidin-4-one; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 3h;

allyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/anie.201507641