3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆

Base Information

Chemical Name:3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆
CAS No.:1266602-57-6
Molecular Formula:C₁₀H₂₂B₆N₂
Molecular Weight:235.164
Hs Code.:

3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB<sub>6</sub>H<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆

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Technology Process of 3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆

There total 1 articles about 3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 67-66-3,8013-54-5
chloroform

: 2001-45-8
tetraphenyl phosphonium chloride

: 6674-22-2,83329-50-4
1,8-diazabicyclo[5.4.0]undec-7-ene

: 1266602-57-6
3-(1,8-diazabicyclo[5.4.0]undec-7-ene)-closo-2-CB₆H₆

: (PPh₄)(3-Cl-closo-2-CB₆H₆)

Guidance literature:: With (TBA)2(B₆H₆); In chloroform; (TBA)2(B6H6) mixed with 1,8-diazabicyclo(5.4.0)undec-7-ene; then CHCl3 added with stirring; stirred under reflux for 17 h; septd.; PPh4Cl in MeCN added to residue; water added; eluated twice with CH2Cl2; org. phase dried with Na2SO4; volatiles removed in vac.; residue suspended in Et2O for 4 times; ppt. filtered; filtrate dried; washed with n-pentane; elem. anal.;
DOI:10.1002/zaac.201000144