rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine)

Base Information

Chemical Name:rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine)
CAS No.:1364512-87-7
Molecular Formula:C₄₃H₃₁Cl₂F₁₀O₃P₂Re
Molecular Weight:1104.76
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine)

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Technology Process of rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine)

There total 1 articles about rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 17442-19-2,80227-22-1
dichlorooxoethoxobis(triphenylphosphine)rhenium(V)

: 38007-33-9
1,1,1,2,2,6,6,7,7,7-decafluoroheptan-3,5-dione

: 1364512-87-7
rhenium dichloro(1,1,1,2,2,6,6,7,7,7-decafluoro-3,5-heptadionate)(triphenylphosphine oxide)(triphenylphosphine)

Guidance literature:: In benzene; Re compd. and ligand (1:1 molar ratio) refluxed for 20 min; octane added, crystd. in 5 d, septd., dried (vac.), elem. anal.;
DOI:10.1134/S1070328412030037