5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Base Information

Chemical Name:5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine
CAS No.:1262838-19-6
Molecular Formula:C₂₃H₃₇N₅O₂
Molecular Weight:415.579
Hs Code.:

Synonyms:

Suppliers and Price of 5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

There total 7 articles about 5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1262838-29-8
2-((3,5-bis(hexyloxy)phenyl)methyl)propanedinitrile

: 50-01-1
guanidine hydrochloride

: 1262838-19-6
5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Guidance literature:: guanidine hydrochloride; With ethanol; sodium; Inert atmosphere;

2-((3,5-bis(hexyloxy)phenyl)methyl)propanedinitrile; In ethanol; for 24h; Reflux; Inert atmosphere;
DOI:10.1246/cl.2010.1166

Reference yield:

: 1262838-28-7
2-((3,5-bis(hexyloxy)phenyl)methylene)propanedinitrile

: 1262838-19-6
5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / isopropyl alcohol / 0.67 h / 0 °C

2.1: ethanol; sodium / Inert atmosphere

2.2: 24 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; ethanol; sodium; In isopropyl alcohol;
DOI:10.1246/cl.2010.1166

Reference yield:

: 111-25-1
1-bromo-hexane

: 1262838-19-6
5-(3,5-bis(hexyloxy)benzyl)-2,4,6-pyrimidinetriamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetonitrile / 13 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 0 °C

3.1: manganese(IV) oxide / dichloromethane / 48 h / 20 °C / Inert atmosphere

4.1: piperidine / ethanol / 0.42 h / Reflux

5.1: sodium tetrahydroborate / isopropyl alcohol / 0.67 h / 0 °C

6.1: ethanol; sodium / Inert atmosphere

6.2: 24 h / Reflux; Inert atmosphere

With piperidine; manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; ethanol; sodium; potassium carbonate; In tetrahydrofuran; ethanol; dichloromethane; isopropyl alcohol; acetonitrile;
DOI:10.1246/cl.2010.1166