C₄₁H₇₇O₂₂P

Base Information

Chemical Name:C₄₁H₇₇O₂₂P
CAS No.:1310568-63-8
Molecular Formula:C₄₁H₇₇O₂₂P
Molecular Weight:953.023
Hs Code.:

C<sub>41</sub>H<sub>77</sub>O<sub>22</sub>P

Synonyms:

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Chemical Property of C₄₁H₇₇O₂₂P

Chemical Property:

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Technology Process of C₄₁H₇₇O₂₂P

There total 10 articles about C₄₁H₇₇O₂₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310568-58-1
C₂₈H₄₈O₁₂

: 1310568-63-8
C₄₁H₇₇O₂₂P

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C

2: 2 h / 160 °C

3: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

4: potassium carbonate; potassium iodide / acetone / 24 h / 60 °C

5: trimethylsilyl bromide / dichloromethane / 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trimethylsilyl bromide; phosphorus tribromide; potassium carbonate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 4: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 1310568-60-5
C₃₂H₅₇O₁₄P

: 1310568-63-8
C₄₁H₇₇O₂₂P

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

2: potassium carbonate; potassium iodide / acetone / 24 h / 60 °C

3: trimethylsilyl bromide / dichloromethane / 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trimethylsilyl bromide; potassium carbonate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 2: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 1310568-63-8
C₄₁H₇₇O₂₂P

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydroxide / tetrahydrofuran; water / 0 - 20 °C

2: potassium carbonate; potassium iodide / acetone / 24 h / 60 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

4: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C

5: 2 h / 160 °C

6: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

7: potassium carbonate; potassium iodide / acetone / 24 h / 60 °C

8: trimethylsilyl bromide / dichloromethane / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trimethylsilyl bromide; phosphorus tribromide; potassium carbonate; potassium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; 2: Williamson reaction / 7: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144