8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Base Information

Chemical Name:8,9-dimethoxy-4-benzylhexahydrobenzoquinoline
CAS No.:72053-28-2
Molecular Formula:C₂₂H₂₅NO₂
Molecular Weight:335.446
Hs Code.:

8,9-dimethoxy-4-benzylhexahydrobenzo<f>quinoline

Synonyms:

Suppliers and Price of 8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

There total 3 articles about 8,9-dimethoxy-4-benzylhexahydrobenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72053-27-1
8,9-dimethoxy-4-benzyl-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

: 72053-28-2
8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene; for 6h; Heating;
DOI:10.1021/jm00175a001

Reference yield:

: 100-39-0
benzyl bromide

: 72053-28-2
8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DME, reflux, 2 h, 2.) DME, reflux, 3 h

2: Red-Al / benzene / 6 h / Heating

With sodium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene;
DOI:10.1021/jm00175a001

Reference yield:

: 72053-26-0
8,9-dimethoxy-1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one

: 72053-28-2
8,9-dimethoxy-4-benzylhexahydrobenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DME, reflux, 2 h, 2.) DME, reflux, 3 h

2: Red-Al / benzene / 6 h / Heating

With sodium hydride; sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene;
DOI:10.1021/jm00175a001