1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine

Base Information

• Chemical Name: 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine
• CAS No.: 82155-32-6
• Molecular Formula: C₃₄H₅₂N₄O₁₈
• Molecular Weight: 804.803

Synonyms:

Chemical Property of 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine

There total 18 articles about 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl azide (69194-62-3) → 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine (82155-32-6,82189-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / PtO₂ (Adam's) / methanol / 3 h

2: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(84)85199-X

Reference yield:

4-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl azide (69194-62-3) → 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine (82155-32-6,82189-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / PtO₂ (Adam's) / methanol / 3 h

2: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(84)85199-X

Reference yield:

BOC-L-aspartic acid 4-benzyl ester (7536-58-5,98482-77-0) → 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine (82155-32-6,82189-31-9)

Guidance literature:

Multi-step reaction with 4 steps

1: N-methylmorpholine, dicyclohexylcarbodiimide / dimethylformamide; CHCl₃ / Ambient temperature

2: 92 percent / hydrogen, 3.5M HCl / Pd black / methanol; dioxane / 5 h

3: dicyclohexylcarbodiimide / dimethylformamide; tetrahydrofuran / 24 h / 0 °C

4: tetrahydrofuran; dimethylformamide / 6 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; hydrogen; dicyclohexyl-carbodiimide; palladium; In tetrahydrofuran; 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(84)85199-X

upstream raw materials:

β-D-cellobiosylamine

(S)-3-tert-Butoxycarbonylamino-N-[(R)-1-((S)-2-hydroxy-1-methoxycarbonyl-ethylcarbamoyl)-2-phenyl-ethyl]-succinamic acid 2,5-dioxo-pyrrolidin-1-yl ester

4-O-(β-D-glucopyranosyl)-β-D-glucopyranosyl azide

BOC-L-aspartic acid 4-benzyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 82155-32-6 1-N--4-O-(β-D-glucopyranosyl)-β-D-glucopyranosylamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send