dimesitylbismuth(III) bromide

Base Information

Chemical Name:dimesitylbismuth(III) bromide
CAS No.:156488-39-0
Molecular Formula:C₁₈H₂₂BiBr
Molecular Weight:527.257
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimesitylbismuth(III) bromide

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Technology Process of dimesitylbismuth(III) bromide

There total 1 articles about dimesitylbismuth(III) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 59344-64-8
tris(2,4,6-trimethylphenyl)bismuth

: 7787-58-8
bismuth(III) bromide

: 156488-39-0
dimesitylbismuth(III) bromide

Guidance literature:: In diethyl ether; dropwise addn. of BiBr3 in Et2O to Bi-compd. in Et2O stirring for 2 h; filtn., washing with ether, drying under reduced pressure, slow evapn. of solns. in Et2O, elem. anal.;
DOI:10.1016/0022-328X(94)80152-5

Reference yield: 100.0%

: 156488-39-0
dimesitylbismuth(III) bromide

: 34669-05-1
ammonium diphenyldithiophosphinate

: 156488-40-3
bis(diphenyldithiophosphinato)mesitylbismuth(III)

Guidance literature:: In benzene; byproducts: NH4Br, NH3, (CH3)3C6H3; refluxing a mixt. of Bi-compd. and NH4PS2Ph2 in anhyd. benzene for 2 h; hot filtn., cooling filtrate to room temp., crystn., filtn., recrystn. from benzene, elem. anal.;
DOI:10.1016/0022-328X(94)80152-5

Reference yield: 77.0%

: 680-31-9
N,N,N,N,N,N-hexamethylphosphoric triamide

: 156488-39-0
dimesitylbismuth(III) bromide

: [Bi(mesityl)2Br(hexamethylphosphoramide)]

Guidance literature:: In dichloromethane; N2-atmosphere; dropwise addn. of excess HMPA to Bi-compd., stirring for 1 h; crystn. on layering with hexanes (-22°C, several weeks); elem. anal.;
DOI:10.1016/0022-328X(95)05474-4