tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Base Information

Chemical Name:tetrakis(2,4,6-trimethylphenyl)dibismuthoxide
CAS No.:165904-01-8
Molecular Formula:C₃₆H₄₄Bi₂O
Molecular Weight:910.706
Hs Code.:

Synonyms:

Suppliers and Price of tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

There total 3 articles about tetrakis(2,4,6-trimethylphenyl)dibismuthoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 146498-75-1
chlorobis(2,4,6-trimethylphenyl)bismuthane

: 80937-33-3
oxygen

: 165904-01-8
tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Guidance literature:: With Na; In ammonia; byproducts: NaCl; NH3 (liquid); Ar-atmosphere; addn. of equimolar amt. of Na to Bi-compd. at -70°C, stirring (-70°C, 4 h); evapn. (0°C), drying (vac., room temp.), stirring in hexane for 30 min, filtration, concn. (vac., 0°C), crystn. (-30°C, 30 h), collection, drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(98)00482-3

Reference yield: 55.0%

: 156488-39-0
dimesitylbismuth(III) bromide

: 1310-73-2
sodium hydroxide

: 165904-01-8
tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Guidance literature:: In diethyl ether; water; byproducts: NaBr; Ar atm., absence of light; equimolar ratio, stirring (2 h); drying (Na2SO4), decantation, evapn. (vac.); elem. anal.;

Reference yield:

: 59344-64-8
tris(2,4,6-trimethylphenyl)bismuth

: 165904-01-8
tetrakis(2,4,6-trimethylphenyl)dibismuthoxide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: Na / ammonia

With Na; In diethyl ether; ammonia;
DOI:10.1016/S0022-328X(98)00482-3