(PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)}

Base Information

Chemical Name:(PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)}
CAS No.:114944-18-2
Molecular Formula:C₁₄H₁₂CoN₂O₂S*C₃₆H₃₀NP₂
Molecular Weight:869.909
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)}

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Technology Process of (PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)}

There total 1 articles about (PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 93473-81-5
(PPN){(η5-cyclopentadienyl)cobalt(cyanide)(CO)}

: 98-59-9
p-toluenesulfonyl chloride

: 114944-18-2
(PPN){(η5-cyclopentadienyl)cobalt(III)(cyanide)2(η1-tosyl)}

Guidance literature:: In tetrahydrofuran; Under N2, cooled soln. (-20°C) of tosyl chloride in THF is added to (PPN)(CpCo(CN)(CO)), mixt. is stirred at -20°C for 2 h , allowed to rise to room temp., stirred for 1 h.; Cooling to -35°C, after 1 d vac. filtn. yields red soln. and green oil, which solidifies when washed with ether. The solid is washed with CH3CN, orange residue is washed with ether and dried on the frit, recrystn. (CH3CN/ether), elem. anal..;