tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide

Base Information

• Chemical Name: tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide
• CAS No.: 852822-63-0
• Molecular Formula: C₂₂H₂₈O₄
• Molecular Weight: 356.462

Synonyms:

Chemical Property of tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide

There total 2 articles about tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopropyl[bis(4-methoxyphenyl)]methanol (111448-45-4) + tert.-butylhydroperoxide (75-91-2) → tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide (852822-63-0)

Guidance literature:

With toluene-4-sulfonic acid; In decane; dichloromethane; at 20 ℃;

DOI:10.1021/jo0502448

Reference yield:

bis(p-methoxyphenyl)methanone (90-96-0) → tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide (852822-63-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: p-toluenesulfonic acid / decane; CH₂Cl₂ / 20 °C

With toluene-4-sulfonic acid; In tetrahydrofuran; decane; dichloromethane;

DOI:10.1021/jo0502448

Reference yield:

tert-butyl cyclopropyl[bis(4-methoxyphenyl)]methyl peroxide (852822-63-0) → cyclopropyl[bis(4-methoxyphenyl)]methoxyl radical (852822-70-9)

Guidance literature:

In acetonitrile; Photolysis;

DOI:10.1021/jo0502448

upstream raw materials:

cyclopropyl[bis(4-methoxyphenyl)]methanol

tert.-butylhydroperoxide

bis(p-methoxyphenyl)methanone

Downstream raw materials:

cyclopropyl[bis(4-methoxyphenyl)]methoxyl radical

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