(3-methyl-2-methylen-3-butenyl)diphenylsilan

Base Information

Chemical Name:(3-methyl-2-methylen-3-butenyl)diphenylsilan
CAS No.:117984-34-6
Molecular Formula:C₂₅H₃₈Si₃
Molecular Weight:422.833
Hs Code.:

<Bis(trimethylsilyl)methyl>(3-methyl-2-methylen-3-butenyl)diphenylsilan

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-methyl-2-methylen-3-butenyl)diphenylsilan

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Technology Process of (3-methyl-2-methylen-3-butenyl)diphenylsilan

There total 14 articles about (3-methyl-2-methylen-3-butenyl)diphenylsilan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117984-08-4
Brom(fluordiphenylsilyl)bis(trimethylsilyl)methan

: 117984-34-6
(3-methyl-2-methylen-3-butenyl)diphenylsilan

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PhLi / 1.) Et₂O, -78 deg C, 2.) 40 deg C

2: 2,3-dimethyl-1,3-butadiene / diethyl ether / 2 h / 100 °C

With phenyllithium; 2,3-dimethyl-buta-1,3-diene; In diethyl ether;

Reference yield:

: 117984-10-8
Brom(bromdiphenylsilyl)bis(trimethylsilyl)methan

: 117984-34-6
(3-methyl-2-methylen-3-butenyl)diphenylsilan

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) PhLi / 1.) Et₂O, -78 deg C, 2.) r.t., 15 h

2: 2,3-dimethyl-1,3-butadiene / diethyl ether / 2 h / 100 °C

With phenyllithium; 2,3-dimethyl-buta-1,3-diene; In diethyl ether;

Reference yield:

: 1631-83-0
diphenylsilyl chloride

: 117984-34-6
(3-methyl-2-methylen-3-butenyl)diphenylsilan

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) Li / 1.) THF, -78 deg C; 2.) THF, -78 deg C, 2 d

2: Br₂ / tetrahydrofuran / -78 °C

3: 96 percent / Br₂ / CCl₄

4: 89 percent / KHF₂ / methanol / 2.5 h / Heating

5: phenyllithium / diethyl ether; benzene / -78 °C

6: 55 percent / diethyl ether / 60 h / 40 °C

7: diethyl ether / 2 h / 100 °C

With potassium hydrogen bifluoride; bromine; lithium; phenyllithium; In tetrahydrofuran; methanol; tetrachloromethane; diethyl ether; benzene;