C₇₃H₁₀₀FNO₁₁

Base Information

• Chemical Name: C₇₃H₁₀₀FNO₁₁
• CAS No.: 1316751-64-0
• Molecular Formula: C₇₃H₁₀₀FNO₁₁
• Molecular Weight: 1186.6
• Mol file: 1316751-64-0.mol

Synonyms:

Chemical Property of C₇₃H₁₀₀FNO₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇₃H₁₀₀FNO₁₁

There total 6 articles about C₇₃H₁₀₀FNO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C50H71N3O9 (1204527-69-4) → C73H100FNO11 (1316751-64-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; triphenylphosphine / water / 16 h / 45 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 16 h / 20 °C

With pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In dichloromethane; water; 1: Staudinger reaction;

DOI:10.1128/AAC.00368-10

Reference yield:

C23H27FO3 → C73H100FNO11 (1316751-64-0)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethylbenzene / 24 h / 20 °C / 760.05 Torr

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 16 h / 20 °C

With palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; ethylbenzene;

DOI:10.1128/AAC.00368-10

Reference yield:

6-O-acetyl-2,3,4-tri-O-benzyl-α/β-D-galactopyranoside (88567-49-1,88567-50-4,93361-01-4,101802-94-2,101802-97-5,127875-38-1) → C73H100FNO11 (1316751-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 2-chloropyridine; dimethylsulfide; trifluoromethylsulfonic anhydride / dichloromethane / 0.67 h / 0 - 20 °C / Molecular sieve; Inert atmosphere

1.2: 16 h / 20 °C / Inert atmosphere

2.1: pyridine; triphenylphosphine / water / 16 h / 45 °C

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 16 h / 20 °C

With pyridine; 2-chloropyridine; dimethylsulfide; trifluoromethylsulfonic anhydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In dichloromethane; water; 2.1: Staudinger reaction;

DOI:10.1128/AAC.00368-10

upstream raw materials:

C₅₀H₇₁N₃O₉

6-O-acetyl-2,3,4-tri-O-benzyl-α/β-D-galactopyranoside

(9-carboxynonyl)triphenylphosphonium bromide

(2S)-2-azido-2-((4S)-2,2-dimethyl-5-tetradecyl-1,3-dioxolan-4-yl)ethan-1-ol