C₂₄H₃₁FN₂O*ClH

Base Information

Chemical Name:C₂₄H₃₁FN₂O*ClH
CAS No.:1356862-18-4
Molecular Formula:C₂₄H₃₁FN₂O*ClH
Molecular Weight:418.982
Hs Code.:

C<sub>24</sub>H<sub>31</sub>FN<sub>2</sub>O*ClH

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₁FN₂O*ClH

Chemical Property:

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Technology Process of C₂₄H₃₁FN₂O*ClH

There total 7 articles about C₂₄H₃₁FN₂O*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₁FN₂O₃

: 1356862-18-4
C₂₄H₃₁FN₂O*ClH

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; ethyl acetate / 16 h / 20 °C / Cooling with ice

2: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 15 h / 20 °C / Cooling with ice

3: hydrogenchloride / water; ethyl acetate

With hydrogenchloride; sodium acetate; sodium tris(acetoxy)borohydride; In dichloromethane; water; ethyl acetate;
DOI:10.1248/cpb.59.1376

Reference yield:

: C₁₅H₂₂FNO₂

: 1356862-18-4
C₂₄H₃₁FN₂O*ClH

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / water; ethyl acetate / 16 h / 20 °C / Cooling with ice

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / acetonitrile / 72 h / 20 °C / Cooling with ice

3: hydrogenchloride / water; ethyl acetate / 16 h / 20 °C / Cooling with ice

4: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 15 h / 20 °C / Cooling with ice

5: hydrogenchloride / water; ethyl acetate

With hydrogenchloride; sodium acetate; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1248/cpb.59.1376

Reference yield:

: C₁₆H₂₃FN₂O*ClH

: 1356862-18-4
C₂₄H₃₁FN₂O*ClH

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 15 h / 20 °C / Cooling with ice

2: hydrogenchloride / water; ethyl acetate

With hydrogenchloride; sodium acetate; sodium tris(acetoxy)borohydride; In dichloromethane; water; ethyl acetate;
DOI:10.1248/cpb.59.1376